Microwave-assisted rapid synthesize of cadmium-thallium mixed fluoride hydrate complex and its physiochemical properties

초록

Herein we report a facile and rapid, cost-effective microwave-assisted synthesis of mixed cadmium-thallium fluoride hydrate compound using a homemade vessel with a special protective outer container. The physico-chemical properties of the prepared compound were investigated by several characterization techniques. Single crystal X-ray diffraction measurement was performed to investigate the crystal structure of the prepared com-pound. The XEOL intensity shows a good linear response as a function of the delivered X-ray dose, which in-dicates that this material can be highly desirable for radiation detection applications. The fitting of scintillation decay kinetic from a241Am & alpha;-radiation source, shows the fastest decay time constant of 40 ns (16%) with medium and slow components of 380 ns (72%) and 1.5 & mu;s (12%) at room temperature. The pulse height spectrum shows the photopeak of & alpha;-particles produced by the 241Am radiation source at 5.48 MeV.

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